全文获取类型
收费全文 | 32118篇 |
免费 | 4025篇 |
国内免费 | 2216篇 |
专业分类
电工技术 | 2654篇 |
技术理论 | 1篇 |
综合类 | 3126篇 |
化学工业 | 4193篇 |
金属工艺 | 2125篇 |
机械仪表 | 2368篇 |
建筑科学 | 2443篇 |
矿业工程 | 1118篇 |
能源动力 | 885篇 |
轻工业 | 2998篇 |
水利工程 | 925篇 |
石油天然气 | 1224篇 |
武器工业 | 482篇 |
无线电 | 3996篇 |
一般工业技术 | 3142篇 |
冶金工业 | 1199篇 |
原子能技术 | 436篇 |
自动化技术 | 5044篇 |
出版年
2024年 | 93篇 |
2023年 | 567篇 |
2022年 | 1284篇 |
2021年 | 1791篇 |
2020年 | 1300篇 |
2019年 | 886篇 |
2018年 | 1029篇 |
2017年 | 1170篇 |
2016年 | 1024篇 |
2015年 | 1577篇 |
2014年 | 2080篇 |
2013年 | 2250篇 |
2012年 | 2712篇 |
2011年 | 2793篇 |
2010年 | 2486篇 |
2009年 | 2357篇 |
2008年 | 2428篇 |
2007年 | 2394篇 |
2006年 | 1953篇 |
2005年 | 1583篇 |
2004年 | 1104篇 |
2003年 | 734篇 |
2002年 | 663篇 |
2001年 | 597篇 |
2000年 | 462篇 |
1999年 | 251篇 |
1998年 | 132篇 |
1997年 | 104篇 |
1996年 | 90篇 |
1995年 | 93篇 |
1994年 | 87篇 |
1993年 | 66篇 |
1992年 | 40篇 |
1991年 | 24篇 |
1990年 | 16篇 |
1989年 | 15篇 |
1988年 | 10篇 |
1987年 | 21篇 |
1986年 | 12篇 |
1985年 | 8篇 |
1984年 | 6篇 |
1983年 | 8篇 |
1982年 | 4篇 |
1981年 | 5篇 |
1980年 | 15篇 |
1979年 | 6篇 |
1974年 | 4篇 |
1970年 | 2篇 |
1959年 | 7篇 |
1951年 | 7篇 |
排序方式: 共有10000条查询结果,搜索用时 83 毫秒
51.
Traditionally, SiC components with complex shapes are very difficult or even impossible to fabricate. This paper aims to develop a new manufacturing process, combining selective laser sintering (SLS), cold isostatic pressing (CIP) and polymer infiltration pyrolysis (PIP), to manufacture complex silicon carbide parts and improve the mechanical properties of silicon carbide ceramic parts. The density and porosity of SiC/SiC composites were measured. Furthermore, the mechanical properties of the specimens with cold isostatic pressing and the specimens without cold isostatic pressing were compared. The bending strength of the specimens with cold isostatic pressing was 201?MPa, and the elastic modulus was 1.27?GPa. And, the bending strength of the specimens without cold isostatic pressing was 142?MPa, and the elastic modulus was 0.88?GPa. Increasing the density of SiC/SiC can enhance the mechanical properties of SiC/SiC composites. 相似文献
52.
Chao Chen Bo Feng Shujuan Hu Yue Zhang Song Li Longfei Gao Xuemei Zhang Kun Yu 《Ceramics International》2018,44(1):216-224
Aluminum phosphate (AlPO4) is a promising oxidation-resistant and weak interface for ceramic-matrix composites. In this research, AlPO4 coating was deposited on mullite fibers by an improved liquid-phase method based on electrostatic attraction. A cationic polyelectrolyte, polyethylenimine (PEI), was used for surface modification of mullite fibers. The formation process, phase evolution and microstructure of the coating were studied. The zeta potential of AlPO4 particles, PEI-adsorbed AlPO4 particles, and PEI-adsorbed mullite particles was characterized to find the proper pH value for improving electrostatic attraction. The obtained AlPO4 coating was porous and continuous, whose thickness could be controlled by multiple coating cycles. The relatively low calcination temperature (600 or 1000 °C) was a useful heat treatment method to develop bonding between coating and fiber as well as reduce the fiber strength degradation. The phase transformations of AlPO4 have little volume change, and cristobalite AlPO4 is thermal compatible with mullite. Therefore, the coating structure was preserved after calcining at 1200 °C. The technique is also applicable for other fibers contained mullite phase to fabricate high-performance AlPO4 coated mullite/mullite composites. 相似文献
53.
54.
目的: 建立快速灵敏的LC-MS/MS法测定人血浆中阿莫西林浓度,并用于两种阿莫西林胶囊的一致性评价。方法: 采用岛津公司LCMS-8060型LC-MS/MS仪,以MRM模式测定阿莫西林(m/z 366.00/114.00)的浓度,d4-阿莫西林作内标(m/z 370.10/114.05),离子源为ESI源。色谱柱选用Waters ACQUITY BEH C18(2.1×50 mm,1.7 μm),梯度洗脱。血浆样本加入内标,经甲醇沉淀蛋白后取上清液进样检测。结果: 所建方法经验证,其线性、准确度、精密度、最低定量限、提取回收率、特异性、基质效应、稳定性等各项指标均符合CFDA的指导原则及最新核查标准要求,并较文献报道中的方法有处理简单、灵敏度高、色谱峰形好的优点。结论: 所建方法快速、灵敏,适用于人血浆中阿莫西林浓度的检测。用于一致性评价的样本实测,两种制剂生物等效。 相似文献
55.
为探究不同表面形貌对粗糙接触界面液体润滑特性的影响,基于有限差分法结合雷诺方程和膜厚方程,研究阶梯形貌、波纹形貌、随机形貌和峡谷形貌4种不同粗糙接触界面液体润滑时的载荷分布及规律。研究发现:4种粗糙表面的三维载荷分布规律都与其表面形貌相对应,在波“峰”处载荷大,摩擦力随载荷的增大而增大,在波“谷”载荷小,摩擦力随载荷减小而减小;4种粗糙表面的载荷随表面展开面积比的变化趋势却有所不同;随表面展开面积比的增大,阶梯形貌表面的载荷呈线性增大,波纹形貌表面的载荷基本不变,随机分布形貌表面的载荷呈增大趋势,峡谷形貌表面的载荷呈先增大后减小的变化趋势。研究结果可以进一步补充现有表面形貌表征和流体润滑等相关研究理论。 相似文献
56.
Peng Jiang Jiafeng Lu Kun Li Xiquan Chen Ruiqi Dan 《Fullerenes, Nanotubes and Carbon Nanostructures》2020,28(5):381-386
AbstractPreparation condition can affect the structure and the properties of nanofiber membrane. In order to explore suitable conditions to prepare the Fe3O4/PVDF nanofiber membrane with good hydrophobicity, the hydrophobicity of Fe3O4/PVDF nanofiber membranes obtained by electrospinning was investigated by changing preparation conditions like weight percentage of Fe3O4 nanoparticles, blending quality concentration of poly (vinylidene fluoride) (PVDF) and Fe3O4 nanoparticles, and positive voltage. And the variations of hydrophobicity of Fe3O4/PVDF nanofiber membranes modified by 1H, 1H, 2H, 2H-perfluorodecyl trimethoxysilane were studied. The results show that the hydrophobicity of Fe3O4/PVDF nanofiber membranes has changed under different preparation conditions. The contact angles of samples increased after a modification by 1H, 1H, 2H, 2H-perfluorodecyl trimethoxysilane, which indicates that the hydrophobicity of Fe3O4/PVDF nanofiber membranes has been enhanced. 相似文献
57.
Yu‐Jung Lin Chun‐Chieh Chen Dang Nguyen Huei‐Rou Su Kun‐Ju Lin Hsin‐Lung Chen Yu‐Jung Hu Po‐Liang Lai Hsing‐Wen Sung 《Small (Weinheim an der Bergstrasse, Germany)》2020,16(23)
Nitric oxide (NO) is a potent tumor‐cell radiosensitizer but it can be readily scavenged by hemoglobin (Hb) in vivo. A biomimetic incubator that can generate and deliver NO in a scavenger (Hb)‐free environment to enhance its radiosensitizing effect to maximize its efficacy in radiotherapy is proposed. This NO incubator comprises a poly(lactic‐co‐glycolic acid) (PLGA) hollow microsphere (HM) that contains an NO donor (NONOate) and a surfactant molecule (sodium caprate, SC) in its aqueous core. In acidic tumorous environments, the PLGA shell of the HM allows the penetration of protons from the outside, activating the hydrolytic cleavage of NONOate, spontaneously generating NO bubbles, which are immediately trapped/stabilized by SC. The SC‐stabilized NO bubbles in the HM are then squeezed through the spaces of its PLGA matrices by the elevated internal pressure. Upon leaving the HM, the entrapped NO molecules may passively diffuse through their SC‐stabilized/protected layer gradually to the tumor site, having a long‐lasting radiosensitizing effect and inhibiting tumor growth. The entire process of NO generation and delivery is conducted in a scavenger (Hb)‐free environment, mimicking the development of young ovoviviparous fish inside their mothers' bodies in the absence of predators before birth. 相似文献
58.
59.
Although Mg alloy possesses high specific strength, low density, and good biocompatibility, poor corrosion resistance hinders its further applications. In the present study, an innovative protective layer against corrosion was prepared on the AZ31 Mg alloy via alkali pretreatment followed by vanillic acid treatment. The alkali pretreatment supplied –OH for the AZ31 Mg alloy surface to react with vanillic acid. The vanillic acid treatment played a crucial role in enhancing the corrosion resistance due to the excellent ability to act as a barrier and retard aqueous solution penetration, which effectively isolated the underlying Mg alloy from the corrosive environment. The corrosion current density of alkali and vanillic acid-treated Mg alloy (AZ31V) almost showed two orders of magnitude lower values in comparison with that of the AZ31 Mg alloy, and the corrosion potential of AZ31V Mg alloy increased from −1.41 to −1.25 V. The immersion tests proved that there was no occurrence of severe corrosion. Hence, the alkali pretreatment and vanillic acid treatment may represent a promising method to improve the corrosion resistance of Mg alloy. 相似文献
60.
随着传感器、数据采集装置和其他具备感知能力的模块在复杂产品服务运行阶段的应用,复杂产品运维系统的数字化和智能化程度越来越高,具有实时、多源、异构、海量等特性的数据成为提高复杂产品系统可靠和低成本运行的决策依据,数字孪生技术提供了一种有效途径。介绍了数据驱动的复杂产品智能服务研究进展;分析了数据驱动的智能服务基本特征与框架模型;提出了数据驱动的复杂产品智能服务方法,主要包括面向服务的复杂产品建模与仿真方法、数据驱动的服务需求获取与精准分析预测方法、基于数字孪生的设备故障识别与动态性能预测方法、数据驱动的装备视情维修与备件库存联合多目标决策优化方法、基于数字孪生的复杂产品辅助维修技术、多要素协同的复杂装备能效精准分析预测方法、基于数据挖掘的复杂产品运行优化控制方法等;给出了智能服务系统的应用案例。所提出的框架和方法可为现代制造服务的智能化转型升级提供参考。 相似文献